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Instrument Equipment
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Quartz Vacuum Chamber
Quartz Vacuum Chamber

Equipment Introduction:

  Overall Structure: The complete set of equipment consists of an electric furnace shell, furnace lining, furnace bottom plate, heating elements, heating element accessories, furnace door and opening mechanism system, and temperature control system.

  Furnace Shell: Parts that come into contact with high temperatures, such as near the furnace door, are made of stainless steel. Heat dissipation protective covers are added to both sides of the furnace body to ensure that the surface temperature rise of the furnace shell is ≤45℃.

  Furnace Chamber: The furnace chamber is entirely constructed using imported composite Morgan alumina fiber materials through a unique numerical control process. It has strong thermal shock resistance, resistance to rapid cooling and heating, good corrosion resistance, no collapse, no crystallization, no slagging, no pollution, and a long service life. This structure features low thermal conductivity, low heat capacity, excellent chemical stability, thermal stability, thermal shock resistance, excellent tensile strength, and corrosion resistance. The fibers can withstand temperatures up to 1500℃. After the lining is completed, a layer of high-temperature curing agent is sprayed onto the surface to form a heat insulation wall, which increases the strength and thermal radiation performance of the lining surface and further reduces heat loss, achieving rapid heating and maximizing the thermal efficiency of the furnace, resulting in good energy-saving effects. The insulation material consists of a composite insulation layer made of high-alumina fiber superhard boards, zirconia-containing high-alumina needle punched blankets, and high-alumina refractory fiber products, providing excellent insulation performance. With a fixed external size of the electric furnace, the furnace chamber volume is indirectly increased by 20%.

  Furnace Accessories: Standard parts, electrical components, and wires all adopt high-quality parts and components from the imported brand Delixi.

Electrical Control System:

  Basic Technical Requirements: The control system must be precise, technologically advanced, functionally complete, have strong anti-interference capabilities, stable operating conditions, and reliable performance. The control cabinet must be well-sealed, finely crafted, aesthetically pleasing, and easy to maintain.

The electrical components inside the electrical control cabinet are all fixed using a skeleton support structure, facilitating inspection and maintenance of the components within the cabinet. It also features good ventilation and heat dissipation to improve the working environment of the electrical components.

  The temperature control system is equipped with PID parameter self-tuning functionality, combining expert modules and control algorithms to achieve precise temperature control and effectively suppress temperature overshoot. It includes a recording curve and a 485 communication interface for connection to a computer. The over-temperature alarm system has the functions of cutting off the main circuit, sound and light alarms, and automatic recovery and release.

  In case of a thermocouple break, the control system can automatically cut off the main circuit power supply and trigger a sound and light alarm.

  Configuration and Structure of the Control Cabinet: The control cabinet is divided into a temperature control unit, a recording unit, an alarm unit, a heating main circuit execution unit, and a mechanical control and safety interlock unit. To ensure the reliability of the control system and highlight its advanced technology, a comprehensive selection of well-known domestic and international brands is used to enhance cost-effectiveness. The main circuit's high-capacity circuit breakers and AC contactors are from the imported brand Delixi. All master switches, buttons, indicator lights, small-capacity circuit breakers, contactors, thermal relays, and thyristor power modules are selected for their reliability and long service life. The trigger and control system should have phase failure detection, over current detection, and alarm reporting functions.

  The three-phase thyristor power module components each adopt an independent forced air-cooled heat dissipation system. The three-phase controlled thyristor power modules are connected in series with AC contactors to prevent uncontrolled heating loops formed by leakage currents in case the thyristor is accidentally punctured, which could lead to temperature runaway. The contactors also cut off the main heating power circuit in the event of thermocouple breakage or over-temperature incidents.

Main Technical Parameter:

  1. furnace effective working dimension:Φ300×400mm

  2. Electrical application total design powerapproximate 4KW

  3. Power supply380V 50Hz

  4. Stainless steel flange

  5. Vacuum tube texturequartz tubeone section closed round bottom

  6. Vacuum systemmolecular pump(KYKY)

  7. Vacuum degree6.67×10-3Pa

Experimental Furnace from Shanghai Institute of Optics and Fine Mechanics, Chinese Academy of Sciences - Quality Advantages:

1. Furnace Shell And Chamber

   Double-layer high-quality carbon steel plate, surface rust resistant high temperature paint treatment;

   Alumina poly-crystalline fiber high temperature furnace, beautiful and energy saving.

2. Electrical Components And Temperature Control

   All electronic components Delixi, thyristor is Japan or Germany original; 

   For safe and efficient use, the use of imported copper isolation transformer; 

   Temperature control and detection are all used: Single platinum rhodium (S type) ≤1500℃; Double platinum rhodium (B type) ≤1800℃

3. Research Team

Senior engineers, master's and doctoral degree holders from the Shanghai Institute of Optics and Fine Mechanics, Chinese Academy of Sciences, are available to assist your company or research institution in selecting the appropriate experimental furnace. Our senior designers will collaborate with you to develop a high-temperature furnace design plan.

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Address:200 Zhaoxian ROAD,JIADING DISTRICT,SHANGHAI 201800,CHINA

Tel:021-69522126

Fax:021-69513319

 

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400-9200-165

Shanghai Institute of Optics and Fine Mechanics.CAS, Chinese Academy of Sciences Opto Electronic Material & Equipment Dept
Address:No. 200 Zhaoxian ROAD,JIADING DISTRICT,SHANGHAI 201800,CHINA Tel:021-69522126 Fax:021-69522153
Technical Support:Qingyun Software